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Study of XRD property matrix by reinforcement of calcium carbonate in different ratio in High density polyethylene
Authors: Gupta Pratibha | Choudary MD | Arajpure VG
Number of views: 344
Polymer exist both in crystalline and amorphous form, polymer crystallinity is one of the most important property of all polymer. Crystallinity of the material is the Presence of amount of crystalline region in polymer with respect to amorphous region, Crystallinity influences most of the polymer properties, some of these are hardness , modulus, stiffness and tensile. X-ray powder diffraction (XRD) is a most commonly used analytical technique for phase identification of a crystalline material and can provide information for the unit cell dimensions. The analyzed material is finely homogenized, ground and average bulk composition is to be determined. X-ray diffraction is also used to measure the nature of polymer and extent of crystallinity present in the polymeric material. Calcium carbonate is used as inorganic filler reinforcement with HDPE as base material with coupling agent, proportionally with eight different proportions. The addition of 5%, 10%, 15%, 20%, 25%, 30%, 35% and 40% on weight fraction basis mixed with HDPE, with the help of an extrusion machine. The resulting mixture characterized by unique microstructure which is responsible for their properties. The reinforcement is stiffer and stronger, than the basic polymer. It increases its modules and strength with change of crystallinity. The objective of the present investigation is to find out the change in microstructure of the composites, and compared with neat material.